amirhosein asilian
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This study addresses the imperative for advanced gas sensors, particularly for monitoring hazardous carbon monoxide (CO), by enhancing nanocrystalline SnO2 thin film fabrication. Control of parameters in the sol-gel synthesis process is systematically explored to mitigate crack formation and enhance SnO2 film quality on uncoated Al2O3 substrates. Leveraging SnO2's n-type semiconductor properties, traditional thin film methods are employed, with a specific focus on overcoming drawbacks through glycerin. Among various fabrication techniques, sol-gel proves cost-effective for producing high-quality, crack-free SnO2 layers tailored for gas sensor applications. The study evaluates sensitivity to CO gas concentrations, improving structural integrity, sensitivity, and stability. X-ray powder diffraction and SEM imaging confirm phase purity and surface morphology, ensuring the absence of impurities or cracks. Integrated with microcontroller-based circuits, the sensors exhibit rapid response and recovery times crucial for real-time gas sensing. The addition of an output circuit with enhanced resolution and stability further enhances sensor performance. Results demonstrate the proposed sensor's capability for rapid response (less than 30 seconds) and recovery times (~39 seconds), crucial for real-time gas sensing. Notably, the sensors demonstrate an admirable sensitivity with a minimum detection limit of as low as 1 ppm of CO gas. Additionally, the study validates the sensor's stability and reliability during prolonged exposure to N2 and 1% CO mixtures, highlighting its potential for personal safety detectors and environmental safety monitoring.
Keywords: Nanocrystalline Sno2, Surface Morphology, Sol-Gel Synthesis, Readout Circuit, Environmental Monitoring.&Lrm -
The unique properties of carbon monoxide and its high combustibility have led to the creation of various sensors, such as electrochemical sensors and different circuits, to read its output. In this article, a deflection-type Wheatstone bridge is used to measure changes in the sensor resistance, and the output voltage is connected to a 12-bit analog-to-digital converter through an adjustable precision amplifier. Next, a new method is proposed for self-calibrating the CO sensor. The Levenberg-Marquardt backpropagation algorithm (LMBP) is utilized in the Artificial Neural Network model to minimize the Mean Squared Error (MSE) and identify the most suitable parameters in the proposed method. The model under consideration has been developed and trained using real-time data. Based on the experimental and evaluation outcomes, it can be concluded that the suggested model has an MSE value of 0.28249 and an R2 coefficient of determination of 0.99992, indicating high accuracy and precision. The proposed sensor and calibration method have potential applications in various applications, including industrial and domestic environments where CO monitoring is necessary.Keywords: Electrochemical sensor, CO monitoring, Levenberg-Marquardt backpropagation algorithm, Mean squared error, Training-Validation, Testing (TVT), coefficient of determination
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