Synthesis and Molecular Structure of [Cd(phen), (NO,)i1

in this research, Complex (o.l(phcnh(N03hl was synthesizcd and the structure was determined by single-crystal X-ray diffraction method. This complex was synthesized by using 1, 10 - Phcnanthrolinc and each of complexes ]Cd(Meurea)61(NO,h and [Cd(urea),(NO,hl at 50-600C. This complex crystallizes in triclinic crystal system, space group P( -. )(2) with two molecules in the unit cell. Laaice parameters of this compound are:a= 9.6008(5)A h= 9.6044(3)A c= 13.4376(1I)A a= 99.5624(4)° (J= 99.5564(6)° y= 105.0862(3)" V= 1152.65(13)A D,",,= 1.7221 mglmchr('39') After structural determination, Rand Rw constants decreased to 0.0772 and 0.0935 respectively. The Cd atom in this complex was eight-coordinated. In addition, If and XRD studies also carried out. -